TA Instruments

AR1697-0001f

04/09/2012 15:01:45

Sample name	ASW 10 mm from base, 60 mm to top, disk 11 PMMA clean
Sample notes	 
Experiment notes	Plastic parallel plate with adaptor supplied by Southampton Uni., on ETC rod with grub screws.

Distances fromlower surface of PP plate. Southampton container.
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1697
Run number	1 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	04/09/2012 15:01:45

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	Yes
Initial temperature	22.4 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:01:00 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 3.000 rad/s
End controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 300.0 rad/s
Duration	0:00:30 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 300.0 rad/s
End controlled variable	velocity 3.000 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	22.4 C
Set temperature system idle	No

Geometry name	25mm ETC plastic plate Southampton
Geometry notes	25 mm diameter parallel plastic plate with ETC rod
Geometry material	Other
Parallel plate diameter	25.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	3.100 micro N.m.s^2
Geometry compliance	2.020E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	1.250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	2.608E5 1/m^3
Fluid density factor	1.278E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	5000 micro m
Approximate sample volume	4.91 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.262 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	3
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	18.42 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Continuous ramp step 1

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

-25.62	7.347	-3.488	1.0040	22.4	99.20	5.2487	10000	0.02435	1.838	6.5608	656.08	3.383E-3	0.0	1.0	61.004	-78.605	5.877
0.9178	14.18	0.06473	2.0160	22.4	93.41	16.1623	10000	0.02293	0.4646	20.203	2020.3	3.383E-3	0.0	1.0	62.016	2.8157	11.34
1.657	20.39	0.08127	3.0080	22.4	97.54	29.5188	10000	0.02394	0.2345	36.899	3689.9	3.383E-3	0.1	1.1	63.008	5.0850	16.31
2.207	23.89	0.09240	3.9920	22.4	90.11	43.3417	10000	0.02212	0.1579	54.177	5417.7	3.384E-3	0.1	1.1	63.992	6.7724	19.11
3.445	31.46	0.1095	5.0080	22.4	85.97	69.9995	10000	0.02110	0.08689	87.499	8749.9	3.384E-3	0.1	1.1	65.008	10.571	25.16
4.583	37.36	0.1227	6.0120	22.4	74.40	97.2321	10000	0.01826	0.05331	121.54	12154	3.383E-3	0.1	1.1	66.012	14.060	29.89
5.992	42.96	0.1395	7.0080	22.4	80.19	128.7350	10000	0.01968	0.04346	160.92	16092	3.383E-3	0.1	1.1	67.008	18.383	34.36
7.445	49.49	0.1505	8.0080	22.4	94.24	168.8890	10000	0.02313	0.03848	211.11	21111	3.384E-3	0.1	1.1	68.008	22.841	39.59
9.955	57.83	0.1721	9.0080	22.4	90.11	225.3140	10000	0.02212	0.02694	281.64	28164	3.383E-3	0.2	1.2	69.008	30.541	46.26
11.71	63.96	0.1831	10.008	22.4	77.71	276.8870	10000	0.01907	0.01900	346.11	34611	3.384E-3	0.2	1.2	70.008	35.927	51.17
13.63	69.89	0.1951	11.008	22.4	77.71	328.2360	10000	0.01907	0.01591	410.30	41030	3.383E-3	0.2	1.2	71.008	41.827	55.92
15.55	75.35	0.2064	12.008	22.4	90.11	379.3760	10000	0.02212	0.01587	474.22	47422	3.383E-3	0.2	1.2	72.008	47.712	60.28
17.26	80.72	0.2138	13.008	22.4	90.93	436.8920	10000	0.02232	0.01395	546.12	54612	3.383E-3	0.2	1.2	73.008	52.947	64.58
19.49	86.63	0.2250	14.012	22.4	80.19	500.7940	10000	0.01968	0.01069	625.99	62599	3.384E-3	0.2	1.2	74.012	59.804	69.30
22.58	94.78	0.2383	15.008	22.4	65.31	596.3770	10000	0.01603	7.269E-3	745.47	74547	3.384E-3	0.3	1.3	75.008	69.285	75.83
24.74	100.1	0.2472	16.008	22.4	79.36	666.4200	10000	0.01948	7.923E-3	833.03	83303	3.384E-3	0.3	1.3	76.008	75.909	80.06
26.99	105.8	0.2550	16.988	22.4	66.13	742.8540	10000	0.01623	5.906E-3	928.57	92857	3.383E-3	0.3	1.3	76.988	82.790	84.66
30.54	113.9	0.2682	18.008	22.4	54.56	857.9490	10000	0.01339	4.207E-3	1072.4	1.0724E5	3.383E-3	0.3	1.3	78.008	93.687	91.10
32.67	119.1	0.2742	19.008	22.4	57.04	940.5220	10000	0.01400	4.018E-3	1175.7	1.1757E5	3.384E-3	0.3	1.3	79.008	100.22	95.32
35.05	124.8	0.2809	20.012	22.4	55.39	1028.6400	10000	0.01359	3.557E-3	1285.8	1.2858E5	3.384E-3	0.3	1.3	80.012	107.54	99.82
37.83	130.2	0.2906	21.008	22.4	39.68	1117.4500	10000	9.739E-3	2.342E-3	1396.8	1.3968E5	3.384E-3	0.4	1.4	81.008	116.05	104.1
41.51	137.8	0.3012	22.008	22.4	38.03	1251.0000	10000	9.333E-3	2.001E-3	1563.8	1.5638E5	3.384E-3	0.4	1.4	82.008	127.37	110.3
44.33	143.3	0.3095	23.008	22.4	45.47	1351.9800	10000	0.01116	2.216E-3	1690.0	1.6900E5	3.383E-3	0.4	1.4	83.008	136.00	114.6
46.82	148.6	0.3150	24.008	22.4	49.60	1453.4100	10000	0.01217	2.245E-3	1816.8	1.8168E5	3.383E-3	0.4	1.4	84.008	143.64	118.9
50.62	156.3	0.3238	25.008	22.4	47.12	1605.3900	10000	0.01156	1.928E-3	2006.7	2.0067E5	3.383E-3	0.4	1.4	85.008	155.31	125.1
52.92	161.7	0.3273	26.012	22.4	23.97	1719.3400	10000	5.884E-3	9.166E-4	2149.2	2.1492E5	3.384E-3	0.4	1.4	86.012	162.37	129.4
56.73	167.1	0.3395	27.008	22.4	13.23	1892.6801	10000	3.246E-3	4.738E-4	2365.9	2.3659E5	3.384E-3	0.5	1.5	87.008	174.03	133.7
61.39	174.8	0.3512	28.008	22.4	19.01	2004.0800	10000	4.666E-3	6.221E-4	2505.1	2.5051E5	3.384E-3	0.5	1.5	88.008	188.35	139.9
63.39	179.9	0.3523	29.008	22.4	14.88	2124.3501	10000	3.652E-3	4.597E-4	2655.4	2.6554E5	3.384E-3	0.5	1.5	89.008	194.48	143.9
67.31	187.9	0.3583	30.008	22.4	28.93	2314.8101	10000	7.101E-3	8.195E-4	2893.5	2.8935E5	3.384E-3	0.5	1.5	90.008	206.52	150.3
70.11	193.0	0.3632	31.008	22.4	19.84	2440.5200	10000	4.869E-3	5.325E-4	3050.7	3.0507E5	3.384E-3	0.5	1.5	91.008	215.09	154.4
73.82	198.1	0.3725	31.996	22.4	20.67	2573.3201	10000	5.072E-3	5.264E-4	3216.7	3.2167E5	3.384E-3	0.5	1.5	91.996	226.48	158.5
78.31	206.1	0.3799	33.012	22.4	9.920	2781.9399	10000	2.435E-3	2.334E-4	3477.4	3.4774E5	3.384E-3	0.6	1.6	93.012	240.24	164.9
81.68	211.3	0.3866	34.008	22.4	-6.613	2921.9600	10000	-1.623E-3	-1.481E-4	3652.5	3.6525E5	3.384E-3	0.6	1.6	94.008	250.60	169.0
86.66	218.9	0.3959	35.008	22.4	3.307	3135.8301	10000	8.116E-4	6.901E-5	3919.8	3.9198E5	3.384E-3	0.6	1.6	95.008	265.87	175.1
89.54	224.2	0.3994	36.008	22.4	-0.8267	3289.0200	10000	-2.029E-4	-1.645E-5	4111.3	4.1113E5	3.384E-3	0.6	1.6	96.008	274.70	179.4
92.92	229.4	0.4051	36.992	22.4	5.787	3439.0801	10000	1.420E-3	1.100E-4	4298.9	4.2989E5	3.384E-3	0.6	1.6	96.992	285.07	183.5
98.09	237.0	0.4139	38.008	22.4	-16.53	3677.2700	10000	-4.058E-3	-2.943E-4	4596.6	4.5966E5	3.383E-3	0.6	1.6	98.008	300.94	189.6
103.2	242.3	0.4259	38.992	22.4	-18.19	3837.1299	10000	-4.464E-3	-3.098E-4	4796.4	4.7964E5	3.383E-3	0.6	1.6	98.992	316.59	193.8
106.2	250.0	0.4248	40.008	22.4	-15.71	4084.2600	10000	-3.855E-3	-2.512E-4	5105.3	5.1053E5	3.384E-3	0.7	1.7	100.008	325.88	200.0
110.8	255.1	0.4343	41.008	22.4	-22.32	4247.4600	10000	-5.478E-3	-3.431E-4	5309.3	5.3093E5	3.384E-3	0.7	1.7	101.008	339.81	204.1
114.6	260.3	0.4401	42.008	22.4	-24.80	4424.2500	10000	-6.087E-3	-3.661E-4	5530.3	5.5303E5	3.383E-3	0.7	1.7	102.008	351.44	208.2
120.8	268.0	0.4507	43.004	22.4	-31.41	4689.5000	10000	-7.710E-3	-4.372E-4	5861.9	5.8619E5	3.383E-3	0.7	1.7	103.004	370.66	214.4
122.8	273.1	0.4496	43.996	22.4	-32.24	4866.0000	10000	-7.913E-3	-4.323E-4	6082.5	6.0825E5	3.384E-3	0.7	1.7	103.996	376.66	218.5
129.8	280.8	0.4622	45.008	22.4	-58.69	5143.7700	10000	-0.01441	-7.446E-4	6429.7	6.4297E5	3.383E-3	0.8	1.8	105.008	398.10	224.6
132.6	285.9	0.4637	46.008	22.4	-48.77	5333.0000	10000	-0.01197	-5.966E-4	6666.3	6.6663E5	3.383E-3	0.8	1.8	106.008	406.73	228.7
135.6	291.0	0.4661	46.992	22.4	-32.24	5522.1899	10000	-7.913E-3	-3.807E-4	6902.7	6.9027E5	3.384E-3	0.8	1.8	106.992	416.10	232.8
142.1	298.7	0.4756	48.008	22.4	-67.79	5818.8501	10000	-0.01664	-7.598E-4	7273.6	7.2736E5	3.384E-3	0.8	1.8	108.008	435.81	239.0
144.1	303.9	0.4741	49.008	22.4	-51.25	6020.7500	10000	-0.01258	-5.550E-4	7525.9	7.5259E5	3.384E-3	0.8	1.8	109.008	442.03	243.1
158.6	311.5	0.5091	50.008	22.4	-120.7	6324.3901	10000	-0.02962	-1.244E-3	7905.5	7.9055E5	3.383E-3	0.8	1.8	110.008	486.49	249.2
165.3	316.5	0.5221	51.008	22.4	-131.4	6531.4902	10000	-0.03226	-1.312E-3	8164.4	8.1644E5	3.384E-3	0.9	1.9	111.008	507.01	253.2
168.1	321.7	0.5224	51.992	22.4	-134.7	6745.9302	10000	-0.03307	-1.302E-3	8432.4	8.4324E5	3.384E-3	0.9	1.9	111.992	515.64	257.4
173.4	329.4	0.5263	52.992	22.4	-135.6	7072.1899	10000	-0.03327	-1.250E-3	8840.2	8.8402E5	3.384E-3	0.9	1.9	112.992	531.85	263.5
177.8	334.4	0.5317	54.008	22.4	-147.1	7282.9502	10000	-0.03611	-1.316E-3	9103.7	9.1037E5	3.383E-3	0.9	1.9	114.008	545.41	267.5
186.2	342.1	0.5444	55.008	22.4	-147.1	7622.5498	10000	-0.03611	-1.257E-3	9528.2	9.5282E5	3.383E-3	0.9	1.9	115.008	571.38	273.7
190.7	347.2	0.5493	56.008	22.4	-170.3	7850.5898	10000	-0.04180	-1.413E-3	9813.2	9.8132E5	3.384E-3	0.9	1.9	116.008	585.09	277.8
195.8	354.7	0.5520	57.008	22.4	-143.0	8196.2998	10000	-0.03510	-1.136E-3	10245	1.0245E6	3.384E-3	1.0	2.0	117.008	600.79	283.8
200.7	359.9	0.5576	57.992	22.4	-201.7	8441.7900	10000	-0.04951	-1.557E-3	10552	1.0552E6	3.384E-3	1.0	2.0	117.992	615.73	287.9
205.8	365.0	0.5637	58.988	22.4	-163.7	8800.8398	10000	-0.04017	-1.228E-3	11001	1.1001E6	3.383E-3	1.0	2.0	118.988	631.33	292.0
216.3	372.6	0.5807	60.008	22.4	-186.8	9034.4102	10000	-0.04585	-1.346E-3	11293	1.1293E6	3.384E-3	1.0	2.0	120.008	663.74	298.0

Peak hold step

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

218.7	375.0	0.5831	1.0000	22.4	-215.8	308.3540	10000	-0.05295	-1.534E-3	385.44	38544	3.383E-3	0.0	2.0	122.000	670.83	300.0
217.3	375.0	0.5796	1.9960	22.4	-224.8	560.7140	10000	-0.05519	-1.599E-3	700.89	70089	3.384E-3	0.0	2.0	122.996	666.75	300.0
216.5	375.0	0.5773	3.0960	22.4	-205.0	936.6300	10000	-0.05032	-1.458E-3	1170.8	1.1708E5	3.384E-3	0.1	2.1	124.096	664.20	300.0
217.5	375.0	0.5799	4.0000	22.4	-223.2	1187.6899	10000	-0.05478	-1.587E-3	1484.6	1.4846E5	3.383E-3	0.1	2.1	125.000	667.17	300.0
216.5	375.0	0.5773	4.9960	22.4	-199.2	1439.0800	10000	-0.04890	-1.417E-3	1798.9	1.7989E5	3.383E-3	0.1	2.1	125.996	664.14	300.0
218.5	375.0	0.5827	6.0160	22.4	-212.4	1816.1600	10000	-0.05214	-1.511E-3	2270.2	2.2702E5	3.384E-3	0.1	2.1	127.016	670.36	300.0
220.1	375.0	0.5870	7.0120	22.4	-213.3	2068.8501	10000	-0.05235	-1.517E-3	2586.1	2.5861E5	3.384E-3	0.1	2.1	128.012	675.31	300.0
219.5	375.0	0.5855	8.0000	22.4	-183.5	2318.6399	10000	-0.04504	-1.305E-3	2898.3	2.8983E5	3.383E-3	0.1	2.2	129.000	673.56	300.0
220.7	375.0	0.5886	9.0160	22.4	-173.6	2695.7100	10000	-0.04261	-1.234E-3	3369.6	3.3696E5	3.384E-3	0.2	2.2	130.016	677.14	300.0
216.6	375.0	0.5775	9.9960	22.4	-171.9	2948.4600	10000	-0.04220	-1.223E-3	3685.6	3.6856E5	3.384E-3	0.2	2.2	130.996	664.46	300.0
219.6	375.0	0.5857	10.996	22.4	-190.1	3198.3899	10000	-0.04666	-1.352E-3	3998.0	3.9980E5	3.383E-3	0.2	2.2	131.996	673.82	300.0
220.4	375.0	0.5877	11.996	22.4	-208.3	3575.4500	10000	-0.05113	-1.481E-3	4469.3	4.4693E5	3.383E-3	0.2	2.2	132.996	676.09	300.0
218.1	375.0	0.5815	12.996	22.4	-192.6	3828.5500	10000	-0.04727	-1.370E-3	4785.7	4.7857E5	3.384E-3	0.2	2.2	133.996	669.07	300.0
220.6	375.0	0.5882	14.004	22.4	-195.9	4204.8101	10000	-0.04809	-1.393E-3	5256.0	5.2560E5	3.384E-3	0.2	2.3	135.004	676.75	300.0
219.6	375.0	0.5856	14.996	22.4	-190.1	4459.5801	10000	-0.04666	-1.352E-3	5574.5	5.5745E5	3.384E-3	0.2	2.3	135.996	673.71	300.0
218.8	375.0	0.5834	15.992	22.4	-196.7	4710.7100	10000	-0.04829	-1.399E-3	5888.4	5.8884E5	3.384E-3	0.3	2.3	136.992	671.23	300.0
222.5	375.0	0.5934	17.012	22.4	-216.6	5083.3398	10000	-0.05316	-1.540E-3	6354.2	6.3542E5	3.383E-3	0.3	2.3	138.012	682.68	300.0
220.2	375.0	0.5873	18.000	22.4	-170.3	5334.7900	10000	-0.04180	-1.211E-3	6668.5	6.6685E5	3.384E-3	0.3	2.3	139.000	675.70	300.0
217.2	375.0	0.5793	18.996	22.4	-160.4	5711.7100	10000	-0.03936	-1.140E-3	7139.6	7.1396E5	3.384E-3	0.3	2.3	139.996	666.46	300.0
219.5	375.0	0.5854	20.000	22.4	-177.7	5964.5698	10000	-0.04362	-1.264E-3	7455.7	7.4557E5	3.384E-3	0.3	2.4	141.000	673.48	300.0
216.8	375.0	0.5781	20.996	22.4	-173.6	6214.2100	10000	-0.04261	-1.234E-3	7767.8	7.7678E5	3.383E-3	0.3	2.4	141.996	665.15	300.0
221.0	375.0	0.5894	21.992	22.4	-200.9	6591.3701	10000	-0.04930	-1.428E-3	8239.2	8.2392E5	3.384E-3	0.4	2.4	142.992	678.12	300.0
223.2	375.0	0.5952	23.000	22.4	-185.2	6842.7402	10000	-0.04545	-1.317E-3	8553.4	8.5534E5	3.384E-3	0.4	2.4	144.000	684.78	300.0
219.5	375.0	0.5854	23.996	22.4	-193.4	7221.2300	10000	-0.04748	-1.376E-3	9026.5	9.0265E5	3.383E-3	0.4	2.4	144.996	673.55	300.0
222.5	375.0	0.5933	25.012	22.4	-191.0	7470.9399	10000	-0.04687	-1.358E-3	9338.7	9.3387E5	3.384E-3	0.4	2.4	146.012	682.60	300.0
222.5	375.0	0.5932	26.012	22.4	-223.2	7722.2100	10000	-0.05478	-1.587E-3	9652.8	9.6528E5	3.384E-3	0.4	2.5	147.012	682.50	300.0
219.9	375.0	0.5863	26.996	22.4	-195.1	8099.3799	10000	-0.04788	-1.387E-3	10124	1.0124E6	3.384E-3	0.4	2.5	147.996	674.51	300.0
218.3	375.0	0.5821	28.000	22.4	-203.4	8355.8301	10000	-0.04991	-1.446E-3	10445	1.0445E6	3.384E-3	0.5	2.5	149.000	669.72	300.0
216.6	375.0	0.5777	28.996	22.4	-190.1	8602.1299	10000	-0.04666	-1.352E-3	10753	1.0753E6	3.383E-3	0.5	2.5	149.996	664.61	300.0
218.8	375.0	0.5834	30.012	22.4	-205.0	8978.9697	10000	-0.05032	-1.458E-3	11224	1.1224E6	3.383E-3	0.5	2.5	151.012	671.25	300.0

Continuous ramp step 2

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

216.3	372.0	0.5813	1.0120	22.4	-183.5	224.8330	10000	-0.04504	-1.326E-3	281.04	28104	3.384E-3	0.0	2.5	152.012	663.49	297.6
209.3	364.5	0.5743	2.0120	22.4	-168.6	581.6330	10000	-0.04139	-1.270E-3	727.04	72704	3.384E-3	0.0	2.6	153.012	642.11	291.6
207.2	359.4	0.5767	3.0240	22.4	-182.7	823.9530	10000	-0.04484	-1.415E-3	1029.9	1.0299E5	3.383E-3	0.1	2.6	154.024	635.79	287.5
197.0	351.7	0.5601	4.0120	22.4	-167.0	1170.4500	10000	-0.04098	-1.350E-3	1463.1	1.4631E5	3.383E-3	0.1	2.6	155.012	604.32	281.3
192.5	346.7	0.5553	5.0080	22.4	-115.7	1395.8000	10000	-0.02840	-9.630E-4	1744.8	1.7448E5	3.384E-3	0.1	2.6	156.008	590.64	277.3
188.6	341.6	0.5521	6.0080	22.4	-115.7	1736.3300	10000	-0.02840	-9.917E-4	2170.4	2.1704E5	3.383E-3	0.1	2.6	157.008	578.66	273.3
180.7	333.9	0.5414	7.0080	22.4	-150.5	1959.3600	10000	-0.03693	-1.350E-3	2449.2	2.4492E5	3.383E-3	0.1	2.6	158.008	554.52	267.1
175.9	328.8	0.5349	8.0080	22.4	-155.4	2173.1599	10000	-0.03814	-1.437E-3	2716.5	2.7165E5	3.384E-3	0.1	2.7	159.008	539.64	263.1
171.2	321.2	0.5331	9.0080	22.4	-147.1	2491.4700	10000	-0.03611	-1.426E-3	3114.3	3.1143E5	3.384E-3	0.2	2.7	160.008	525.33	257.0
166.1	316.1	0.5255	10.012	22.4	-142.2	2704.1699	10000	-0.03490	-1.423E-3	3380.2	3.3802E5	3.383E-3	0.2	2.7	161.012	509.55	252.9
158.1	308.4	0.5128	11.012	22.4	-112.4	3010.9900	10000	-0.02759	-1.182E-3	3763.7	3.7637E5	3.384E-3	0.2	2.7	162.012	485.20	246.7
154.3	303.3	0.5086	12.008	22.4	-108.3	3211.1599	10000	-0.02658	-1.177E-3	4014.0	4.0140E5	3.384E-3	0.2	2.7	163.008	473.32	242.7
150.2	298.2	0.5038	13.012	22.4	-108.3	3412.4199	10000	-0.02658	-1.218E-3	4265.5	4.2655E5	3.384E-3	0.2	2.7	164.012	460.90	238.5
143.3	290.5	0.4933	14.008	22.4	-66.13	3699.3401	10000	-0.01623	-7.835E-4	4624.2	4.6242E5	3.383E-3	0.2	2.8	165.008	439.70	232.4
140.5	285.5	0.4920	15.016	22.4	-105.8	3888.7000	10000	-0.02597	-1.299E-3	4860.9	4.8609E5	3.384E-3	0.3	2.8	166.016	430.92	228.4
134.4	277.7	0.4840	16.008	22.4	-59.52	4169.8799	10000	-0.01461	-7.716E-4	5212.4	5.2124E5	3.383E-3	0.3	2.8	167.008	412.42	222.2
130.9	272.6	0.4801	17.008	22.4	-76.05	4349.9902	10000	-0.01867	-1.024E-3	5437.5	5.4375E5	3.383E-3	0.3	2.8	168.008	401.45	218.0
124.6	265.0	0.4701	18.012	22.4	-47.95	4612.5601	10000	-0.01177	-6.827E-4	5765.7	5.7657E5	3.383E-3	0.3	2.8	169.012	382.23	212.0
121.6	259.8	0.4680	19.008	22.4	-57.87	4787.7700	10000	-0.01420	-8.571E-4	5984.7	5.9847E5	3.383E-3	0.3	2.8	170.008	373.05	207.9
116.5	254.6	0.4576	20.008	22.4	-33.89	4962.7998	10000	-8.319E-3	-5.230E-4	6203.5	6.2035E5	3.384E-3	0.3	2.9	171.008	357.40	203.7
111.2	247.0	0.4502	21.008	22.4	-52.91	5208.0298	10000	-0.01299	-8.675E-4	6510.0	6.5100E5	3.383E-3	0.4	2.9	172.008	341.10	197.6
109.0	241.8	0.4506	22.008	22.4	-44.64	5369.1899	10000	-0.01096	-7.635E-4	6711.5	6.7115E5	3.383E-3	0.4	2.9	173.008	334.27	193.4
103.6	234.0	0.4429	23.004	22.4	-47.12	5607.0098	10000	-0.01156	-8.607E-4	7008.8	7.0088E5	3.383E-3	0.4	2.9	174.004	317.91	187.2
100.2	229.0	0.4375	24.008	22.4	-33.89	5756.7798	10000	-8.319E-3	-6.465E-4	7196.0	7.1960E5	3.384E-3	0.4	2.9	175.008	307.34	183.2
96.79	223.8	0.4324	25.024	22.4	-31.41	5906.7100	10000	-7.710E-3	-6.270E-4	7383.4	7.3834E5	3.384E-3	0.4	2.9	176.024	296.93	179.1
89.27	215.9	0.4134	26.008	22.4	-12.40	6131.6499	10000	-3.043E-3	-2.660E-4	7664.6	7.6646E5	3.383E-3	0.4	3.0	177.008	273.87	172.7
86.90	210.8	0.4122	27.008	22.4	-28.93	6269.1299	10000	-7.101E-3	-6.510E-4	7836.4	7.8364E5	3.383E-3	0.5	3.0	178.008	266.59	168.7
82.18	203.1	0.4046	28.008	22.4	-1.45E-11	6475.2500	10000	-3.55E-15	-3.51E-16	8094.1	8.0941E5	3.383E-3	0.5	3.0	179.008	252.14	162.5
78.19	197.8	0.3952	29.008	22.4	-22.32	6612.6201	10000	-5.478E-3	-5.703E-4	8265.8	8.2658E5	3.384E-3	0.5	3.0	180.008	239.88	158.3
75.84	192.5	0.3940	30.008	22.4	-15.71	6743.6699	10000	-3.855E-3	-4.239E-4	8429.6	8.4296E5	3.384E-3	0.5	3.0	181.008	232.67	154.0
70.15	184.8	0.3795	31.008	22.4	-0.8267	6930.9502	10000	-2.029E-4	-2.420E-5	8663.7	8.6637E5	3.384E-3	0.5	3.0	182.008	215.22	147.9
66.66	179.5	0.3713	32.008	22.4	9.920	7055.7402	10000	2.435E-3	3.078E-4	8819.7	8.8197E5	3.383E-3	0.5	3.1	183.008	204.51	143.6
63.61	174.2	0.3651	33.008	22.4	25.63	7175.7300	10000	6.290E-3	8.445E-4	8969.7	8.9697E5	3.384E-3	0.6	3.1	184.008	195.14	139.4
59.79	166.6	0.3590	34.008	22.4	9.093	7342.7002	10000	2.232E-3	3.278E-4	9178.4	9.1784E5	3.384E-3	0.6	3.1	185.008	183.44	133.2
57.18	161.3	0.3546	35.008	22.4	14.88	7454.9102	10000	3.652E-3	5.722E-4	9318.6	9.3186E5	3.384E-3	0.6	3.1	186.008	175.42	129.0
54.04	153.4	0.3522	36.008	22.4	15.71	7611.5698	10000	3.855E-3	6.671E-4	9514.5	9.5145E5	3.384E-3	0.6	3.1	187.008	165.80	122.8
49.33	148.3	0.3326	37.008	22.4	29.76	7710.5898	10000	7.304E-3	1.353E-3	9638.2	9.6382E5	3.384E-3	0.6	3.1	188.008	151.33	118.7
46.08	143.0	0.3222	38.008	22.4	43.81	7810.2402	10000	0.01075	2.142E-3	9762.8	9.7628E5	3.384E-3	0.6	3.2	189.008	141.36	114.4
42.08	134.9	0.3120	39.008	22.4	34.72	7953.8999	10000	8.521E-3	1.908E-3	9942.4	9.9424E5	3.384E-3	0.7	3.2	190.008	129.10	107.9
39.54	129.8	0.3047	40.008	22.4	34.72	8040.5098	10000	8.521E-3	2.061E-3	10051	1.0051E6	3.384E-3	0.7	3.2	191.008	121.32	103.8
38.09	124.5	0.3060	41.008	22.4	47.12	8127.6401	10000	0.01156	3.041E-3	10160	1.0160E6	3.384E-3	0.7	3.2	192.008	116.86	99.59
35.42	116.3	0.3046	42.008	22.4	43.81	8253.4902	10000	0.01075	3.239E-3	10317	1.0317E6	3.384E-3	0.7	3.2	193.008	108.67	93.04
31.89	111.2	0.2867	43.008	22.4	51.25	8326.5195	10000	0.01258	4.143E-3	10408	1.0408E6	3.384E-3	0.7	3.2	194.008	97.842	88.98
29.16	105.9	0.2753	44.008	22.4	52.08	8401.0996	10000	0.01278	4.643E-3	10501	1.0501E6	3.384E-3	0.7	3.3	195.008	89.459	84.73
26.17	100.3	0.2609	45.008	22.4	62.00	8475.5000	10000	0.01522	6.160E-3	10594	1.0594E6	3.383E-3	0.8	3.3	196.008	80.302	80.26
23.26	92.10	0.2526	46.008	22.4	62.83	8574.7402	10000	0.01542	7.407E-3	10718	1.0718E6	3.384E-3	0.8	3.3	197.008	71.368	73.68
20.81	86.73	0.2399	47.008	22.4	71.92	8636.6396	10000	0.01765	9.560E-3	10796	1.0796E6	3.384E-3	0.8	3.3	198.008	63.843	69.39
18.80	81.02	0.2321	48.008	22.4	70.27	8699.4297	10000	0.01725	0.01070	10874	1.0874E6	3.384E-3	0.8	3.3	199.008	57.684	64.82
16.33	75.22	0.2171	49.008	22.4	66.96	8754.3096	10000	0.01643	0.01183	10943	1.0943E6	3.383E-3	0.8	3.3	200.008	50.102	60.17
13.58	67.16	0.2022	50.008	22.4	85.97	8828.0703	10000	0.02110	0.01906	11035	1.1035E6	3.384E-3	0.8	3.4	201.008	41.656	53.73
11.70	61.23	0.1912	51.008	22.4	80.19	8877.1797	10000	0.01968	0.02139	11096	1.1096E6	3.384E-3	0.9	3.4	202.008	35.907	48.98
9.763	55.11	0.1772	52.008	22.4	76.88	8920.3604	10000	0.01887	0.02531	11150	1.1150E6	3.384E-3	0.9	3.4	203.008	29.953	44.09
8.463	49.67	0.1704	53.008	22.4	79.36	8956.8896	10000	0.01948	0.03217	11196	1.1196E6	3.383E-3	0.9	3.4	204.008	25.964	39.74
6.593	43.60	0.1512	54.008	22.4	82.67	8993.3301	10000	0.02029	0.04349	11242	1.1242E6	3.384E-3	0.9	3.4	205.008	20.226	34.88
4.929	37.24	0.1324	55.008	22.4	90.11	9023.5898	10000	0.02212	0.06497	11279	1.1279E6	3.384E-3	0.9	3.4	206.008	15.122	29.79
3.798	31.80	0.1194	56.008	22.4	75.23	9047.9004	10000	0.01846	0.07438	11310	1.1310E6	3.384E-3	0.9	3.5	207.008	11.652	25.44
2.592	25.32	0.1024	57.016	22.4	95.89	9071.4102	10000	0.02354	0.1496	11339	1.1339E6	3.383E-3	1.0	3.5	208.016	7.9518	20.26
1.502	18.12	0.08290	58.004	22.4	102.5	9088.7803	10000	0.02516	0.3123	11361	1.1361E6	3.384E-3	1.0	3.5	209.004	4.6080	14.49
0.7744	12.21	0.06341	59.036	22.4	103.3	9100.0400	10000	0.02536	0.6928	11375	1.1375E6	3.384E-3	1.0	3.5	210.036	2.3759	9.770
0.3984	8.121	0.04907	60.008	22.4	87.62	9104.9600	10000	0.02151	1.329	11381	1.1381E6	3.384E-3	1.0	3.5	211.008	1.2224	6.497

